An Undergraduate Experiment Using Microwave-Assisted Synthesis of Metalloporphyrins: Characterization and Spectroscopic Investigations

Shaikha S. Al Neyadi; Ahmed Alzamly; Abdullah Al-Hemyari; Ibrahim M. Tahir; Saeed Al-Meqbali; M. A.Ali Ahmad; Muna Bufaroosha

doi:10.12691/wjce-7-1-4

An Undergraduate Experiment Using Microwave-Assisted Synthesis of Metalloporphyrins: Characterization and Spectroscopic Investigations

Shaikha S. Al Neyadi, Ahmed Alzamly, Abdullah Al-Hemyari, Ibrahim M. Tahir, Saeed Al-Meqbali, M. A.Ali Ahmad, Muna Bufaroosha

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

Abstract

The effectiveness of microwave-assisted synthesis of 5,10,15,20-tetraphenylporphyrin and its corresponding to metal complexes of (Bi (III), Zn (II) and Ni (II)) are described. Moreover, the synthesized metalloporphyrins that were obtained with reasonable yields were characterized using UV-vis, ¹H-NMR and IR.

Original language	English
Pages (from-to)	26-32
Number of pages	7
Journal	World Journal of Chemical Education
Volume	7
Issue number	1
DOIs	https://doi.org/10.12691/wjce-7-1-4
Publication status	Published - 2019

Keywords

metalloporphyrins
microwave synthesis
porphyrins

ASJC Scopus subject areas

Analytical Chemistry
Chemistry (miscellaneous)
Education
Physical and Theoretical Chemistry

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10.12691/wjce-7-1-4

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title = "An Undergraduate Experiment Using Microwave-Assisted Synthesis of Metalloporphyrins: Characterization and Spectroscopic Investigations",

abstract = "The effectiveness of microwave-assisted synthesis of 5,10,15,20-tetraphenylporphyrin and its corresponding to metal complexes of (Bi (III), Zn (II) and Ni (II)) are described. Moreover, the synthesized metalloporphyrins that were obtained with reasonable yields were characterized using UV-vis, 1H-NMR and IR.",

keywords = "metalloporphyrins, microwave synthesis, porphyrins",

author = "{Al Neyadi}, {Shaikha S.} and Ahmed Alzamly and Abdullah Al-Hemyari and Tahir, {Ibrahim M.} and Saeed Al-Meqbali and Ahmad, {M. A.Ali} and Muna Bufaroosha",

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year = "2019",

doi = "10.12691/wjce-7-1-4",

language = "English",

volume = "7",

pages = "26--32",

journal = "World Journal of Chemical Education",

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TY - JOUR

T1 - An Undergraduate Experiment Using Microwave-Assisted Synthesis of Metalloporphyrins

T2 - Characterization and Spectroscopic Investigations

AU - Al Neyadi, Shaikha S.

AU - Alzamly, Ahmed

AU - Al-Hemyari, Abdullah

AU - Tahir, Ibrahim M.

AU - Al-Meqbali, Saeed

AU - Ahmad, M. A.Ali

AU - Bufaroosha, Muna

N1 - Publisher Copyright: © The Author(s) 2019

PY - 2019

Y1 - 2019

N2 - The effectiveness of microwave-assisted synthesis of 5,10,15,20-tetraphenylporphyrin and its corresponding to metal complexes of (Bi (III), Zn (II) and Ni (II)) are described. Moreover, the synthesized metalloporphyrins that were obtained with reasonable yields were characterized using UV-vis, 1H-NMR and IR.

AB - The effectiveness of microwave-assisted synthesis of 5,10,15,20-tetraphenylporphyrin and its corresponding to metal complexes of (Bi (III), Zn (II) and Ni (II)) are described. Moreover, the synthesized metalloporphyrins that were obtained with reasonable yields were characterized using UV-vis, 1H-NMR and IR.

KW - metalloporphyrins

KW - microwave synthesis

KW - porphyrins

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UR - http://www.scopus.com/inward/citedby.url?scp=85073814124&partnerID=8YFLogxK

U2 - 10.12691/wjce-7-1-4

DO - 10.12691/wjce-7-1-4

M3 - Article

AN - SCOPUS:85073814124

SN - 2375-1665

VL - 7

SP - 26

EP - 32

JO - World Journal of Chemical Education

JF - World Journal of Chemical Education

IS - 1

ER -

An Undergraduate Experiment Using Microwave-Assisted Synthesis of Metalloporphyrins: Characterization and Spectroscopic Investigations

Abstract

Keywords

ASJC Scopus subject areas

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